The TGA weight modify curve is shown in Figure 1. The primary weight loss move is the volatilization followed by a major decomposition phase. The derivative of bodyweight alter curve in inexperienced displays a peak where the height max is at 427.71 ˚C. The MS data is gathered through the whole TGA experiment. Ion currents and TGA mass loss are plotted being a functionality of temperature (see Determine two). It is important to bear in mind the merchandise of the TGA examination are Generally decomposition products, and that's correct in these experiments likewise. Consequently, the purpose is to be aware of the thermal degradation products of nylon sixty six. TGA-MS consistently monitors the decomposition off gases to be a operate of your time and temperature. The degradation mechanism of the polymer molecules breaking at the C-N bond creates smaller polymer molecules Along with the exact same device of bicarbonyl polymethylene fragments along with the fragments will stop working into carbon dioxide, carbon monoxide, h2o, and hydrocarbons [five].
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TGA-FTIR spectra were being recorded over the TGA examination as being a operate of your time and stored within an array given that the Gram Schmidt file at Every knowledge stage
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The degradation of nylon sixty six in this Section of the study was also completed on the TGA5500. The off-gas merchandise ended up analyzed using a FTIR to the IR spectra and also a GC/MS for the MS Evaluation.